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1 H NMR (600 MHz, CD 3 OD) 6.26 (app s, 1 H), 6.25 (app d, J = 1.9 Hz, 1 H), 5.70 (dd, J = 5.0, 6.9 Hz, 1 H), 4.48 (ddd, J = 5.0, 7.0, 11.8 Hz, 1 H), 3.54 (dd, J = 6.9, 12.2 Hz, 1 H), 3.48 (app td, J = 7.6, 11.8 Hz, 1 H), 3.38 (ddd, J = 6.5, 8.2, 11.8 Hz, 1 H), 3.27 (dd, J = 4.7, 12.2 Hz, 1 H), 2.34 (ddd, J = 7.3, 14.0, 15.2 Hz, 1 H), 2.06 (app ddt, J = 1.4, 6.8, 13.2 Hz, 1 H)

Proceedings of the National Academy of Sciences